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Flow electrochemical cyclizations via amidyl radicals: easy access to cyclic ureas

Ahmed, Nisar and Vgenopoulou, Aggeliki 2019. Flow electrochemical cyclizations via amidyl radicals: easy access to cyclic ureas. SynOpen 03 (01) , pp. 46-48. 10.1055/s-0037-1611772

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Abstract

Flow chemistry has advantages over batch processes and can achieve the synthesis of substances in high yield under safe working conditions. The combination of electrochemistry and flow microreactor technology has made chemical transformations possible without the use of oxidants or catalysts. Herein, we report flow electrosynthesis of cyclic ureas via oxyamination of N-allylic ureas. We have found that continuous flow is able to outperform its batch counterpart, producing cyclic ureas in excellent yields.

Item Type: Article
Date Type: Publication
Status: Published
Schools: Chemistry
ISSN: 2509-9396
Date of First Compliant Deposit: 25 February 2021
Date of Acceptance: 3 March 2019
Last Modified: 25 Feb 2021 15:00
URI: http://orca.cardiff.ac.uk/id/eprint/138945

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