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Dimethylaluminium methylselenolate

Choi, Joong-Kwon, Shahzad, Sohail Anjum and Wirth, Thomas 2009. Dimethylaluminium methylselenolate. In: Paquette, Leo A. ed. Encyclopedia of reagents for organic synthesis (e-EROS), Chichester: Wiley, (10.1002/047084289X.rd300.pub2)

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(preparation of methyl selenoesters; aldol condensation of enones) Solubility: reaction are typically run in toluene. Preparative Methods: conveniently prepared by heating a toluene solution of Trimethylaluminum with powdered Selenium for 2 h at reflux.2 The yellow-colored supernatant was transferred to a septum-capped argon-filled Erlenmeyer flask. Handling, Storage, and Precautions: the reagent was found to retain its activity for approximately one month at rt. Selenium reagents are toxic and should be handled with caution, in a fume hood.

Item Type: Book Section
Date Type: Publication
Status: Published
Schools: Chemistry
Subjects: Q Science > QD Chemistry
Publisher: Wiley
ISBN: 9780470842898
Last Modified: 04 Jun 2017 03:40

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