Preparation of oxonanes and azonanes by oxidative ring expansion: synthesis of obtusan

Brown, David S., Elliott, Mark Christopher ORCID: https://orcid.org/0000-0003-0132-0818, Moody, Christopher J. and Mowlem, Timothy J. 1995. Preparation of oxonanes and azonanes by oxidative ring expansion: synthesis of obtusan. Journal of the Chemical Society, Perkin Transactions 1 1995 (9) , pp. 1137-1144. 10.1039/p19950001137

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Abstract

Oxonanes can be readily prepared from phthalans by a 3-step procedure involving Birch reduction, selective hydrogenation and oxidation. 2-Ethyl-9-pentyloxonane-3,8-dione has been deoxygenated to give obtusan. The method has been applied to the synthesis of an azonane.

Item Type:	Article
Date Type:	Publication
Status:	Published
Schools:	Schools > Chemistry
Subjects:	Q Science > QD Chemistry
Publisher:	RSC Publishing
ISSN:	0300-922X
Last Modified:	21 Oct 2022 10:21
URI:	https://orca.cardiff.ac.uk/id/eprint/39952

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