Flow synthesis of symmetrical di- and trisulfides using phase-transfer catalysis

Baker, Alastair Richard ORCID: https://orcid.org/0000-0003-0857-6533, Graz, Michael, Saunders, Robert, Evans, Gareth J. S., Kaul, Sandra and Wirth, Thomas ORCID: https://orcid.org/0000-0002-8990-0667 2013. Flow synthesis of symmetrical di- and trisulfides using phase-transfer catalysis. Journal of Flow Chemistry 3 (4) , pp. 118-121. 10.1556/JFC-D-13-00013

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Abstract

Using mild conditions and short reaction times, symmetrical disulfides have been synthesized in flow chemistry using phase transfer catalysts to facilitate the substitution of organohalides with disodium disulfide. Also, the synthesis of symmetrical trisulfides was possible using this procedure with an additional equivalent of sulfur.

Item Type:	Article
Date Type:	Publication
Status:	Published
Schools:	Chemistry
Subjects:	Q Science > QD Chemistry
Uncontrolled Keywords:	flow chemistry; phase transfer catalysts; symmetrical disulfides; symmetrical trisulfides
Publisher:	Akademiai Kiado
ISSN:	2062-249X
Last Modified:	25 Oct 2022 09:03
URI:	https://orca.cardiff.ac.uk/id/eprint/57074

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