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Total synthesis of (+)-crocacin C

Dias, Luiz C. and Gonzaga De Oliveira, Luciana 2001. Total synthesis of (+)-crocacin C. Organic Letters 3 (24) , pp. 3951-3954. 10.1021/ol016845c

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The total synthesis of (+)-crocacin C is described. The convergent asymmetric synthesis relies on the use of a regio- and diastereoselective epoxidation of an allylic alcohol with m-CPBA followed by epoxide opening with Me2CuCNLi2 and a Stille cross-coupling between E-vinyl stannane 5 and E-vinyl iodide 6 to establish the (E,E)-dienamide moiety.

Item Type: Article
Date Type: Publication
Status: Published
Schools: Chemistry
Publisher: American Chemical Society
ISSN: 1523-7060
Last Modified: 14 Nov 2022 16:04

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