XPS analysis of electrically insulating catalytic materials

Morgan, David J. ORCID: https://orcid.org/0000-0002-6571-5731 2023. XPS analysis of electrically insulating catalytic materials. Zafeiratos, Spyridon, ed. Applications of X-ray Photoelectron Spectroscopy to Catalytic Studies: From Routine Analysis to Cutting-Edge Surface Characterization, Catalytic Science Series: Volume 21, World Scientific, pp. 97-120. (10.1142/9781800613294_0005)

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Abstract

Due to the highly insulating nature of most catalytic samples, some form of charge compensation is required to study such samples by X-ray photoelectron spectroscopy (XPS). This chapter provides an overview of charge build-up at surfaces and how such phenomena may be overcome, enabling the analyst to obtain meaningful spectral shapes and binding energies from the recorded photoelectron spectra. An overview of the variety of approaches used for charge correction in the literature is presented, with a critical view towards their use in catalytic materials.

Item Type:	Book Section
Date Type:	Publication
Status:	Published
Schools:	Cardiff Catalysis Institute (CCI) Chemistry
Publisher:	World Scientific
ISBN:	9781800613294
Last Modified:	25 Aug 2023 09:26
URI:	https://orca.cardiff.ac.uk/id/eprint/161975

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