Exploiting in situ solid-state NMR for the discovery of new polymorphs during crystallization processes

Hughes, Colan Evan, Williams, Philip Andrew, Peskett, Thomas Roper and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2012. Exploiting in situ solid-state NMR for the discovery of new polymorphs during crystallization processes. The Journal of Physical Chemistry Letters 3 (21) , pp. 3176-3181. 10.1021/jz301252u

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Abstract

We report the discovery of new polymorphic forms of solids by exploiting a solid-state NMR technique that has been developed for in situ monitoring of the evolution of crystallization processes. The capability of the technique to reveal the existence of new polymorphic forms of molecular solids is illustrated by the discovery of two new polymorphs of methyldiphenylphosphine oxide and a new solid form of the 1,10-dihydroxydecane/urea system.

Item Type:	Article
Date Type:	Publication
Status:	Published
Schools:	Chemistry
Subjects:	Q Science > QD Chemistry
Uncontrolled Keywords:	crystallization; polymorphism; in situ techniques; solid-state NMR
Publisher:	ACS Publications
ISSN:	1948-7185
Last Modified:	21 Oct 2022 10:38
URI:	https://orca.cardiff.ac.uk/id/eprint/40863

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