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Towards microfluidic reactors for in situ synchrotron infrared studies

Silverwood, I. P., Al-Rifai, N., Cao, E., Nelson, D. J., Chutia, A., Wells, P. P., Nolan, S. P., Frogley, M. D., Cinque, G., Gavriilidis, A. and Catlow, Charles Richard ORCID: 2016. Towards microfluidic reactors for in situ synchrotron infrared studies. Review of Scientific Instruments 87 (2) , 024101. 10.1063/1.4941825

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Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described.

Item Type: Article
Date Type: Publication
Status: Published
Schools: Cardiff Catalysis Institute (CCI)
Subjects: Q Science > QD Chemistry
Publisher: American Institute of Physics
ISSN: 0034-6748
Date of Acceptance: 28 January 2016
Last Modified: 01 Nov 2022 10:20

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