Hughes, Colan E, Williams, Andrew, Kariuki, Benson M ![]() ![]() |
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Abstract
With the growing realization that crystallization processes may evolve through a sequence of different solid forms, including amorphous precursor phases, the development of suitable in situ experimental probes is essential for comprehensively mapping the time‐evolution of such processes. Here we demonstrate that the CLASSIC NMR (Combined Liquid‐ And Solid‐State In situ Crystallization NMR) strategy is a powerful technique for revealing the transitory existence of amorphous phases during crystallization processes, applying this technique to study crystallization of DL menthol and L menthol from their molten liquid phases. The CLASSIC NMR results provide direct insights into the conditions (including the specific time period) under which the molten liquid phase, transitory amorphous phases and final crystalline phases exist during these crystallization processes.
Item Type: | Article |
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Date Type: | Publication |
Status: | Published |
Schools: | Chemistry Advanced Research Computing @ Cardiff (ARCCA) |
Publisher: | Wiley-VCH Verlag |
ISSN: | 1439-4235 |
Date of First Compliant Deposit: | 23 October 2018 |
Date of Acceptance: | 22 October 2018 |
Last Modified: | 08 Nov 2023 11:05 |
URI: | https://orca.cardiff.ac.uk/id/eprint/116121 |
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