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Palladium-catalyzed allylic fluorination

Hollingworth, Charlotte, Hazari, Amaruka, Hopkinson, Matthew N., Tredwell, Matthew ORCID:, Benedetto, Elena, Huiban, Mickael, Gee, Antony D., Brown, John M. and Gouverneur, Veronique 2011. Palladium-catalyzed allylic fluorination. Angewandte Chemie International Edition 50 (11) , pp. 2613-2617. 10.1002/anie.201007307

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The title reaction is presented and its applicability to 18F radiolabeling is demonstrated (see scheme; TBAF=tetra‐n‐butylammonium fluoride, THF=tetrahydrofuran, dba=dibenzylideneacetone). The use of p‐nitrobenzoate as the leaving group is significant to the success of this catalytic organometallic fluorination process. A range of allylic fluorides were synthesized by this method.

Item Type: Article
Date Type: Published Online
Status: Published
Schools: Medicine
Publisher: Wiley
ISSN: 1433-7851
Last Modified: 04 Nov 2022 12:11

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