A superior procedure for generation of substituted benzyllithiums from the corresponding chlorides

Smith, Keith and Hou, Duanjie 1995. A superior procedure for generation of substituted benzyllithiums from the corresponding chlorides. Journal of the Chemical Society, Perkin Transactions 1 (3) , pp. 185-186. 10.1039/P19950000185

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Abstract

The use of diethyl ether–tetrahydrofuran–light petroleum (b.p. 30–40 °C)(4:3:1) as solvent for the reaction of substituted benzyl chlorides with lithium naphthalenide at low temperature gives useful yields of the corresponding benzyllithium compounds, which react with electrophiles such as iodomethane and water to yield the expected reaction products.

Item Type:	Article
Status:	Published
Schools:	Chemistry
Subjects:	Q Science > QD Chemistry
Publisher:	RSC Publishing
ISSN:	0300-922X
Last Modified:	04 Jun 2017 02:51
URI:	https://orca.cardiff.ac.uk/id/eprint/12688

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