Selective transformation pathways between crystalline forms of an organic material established from powder X-ray diffraction analysis

Fujii, Kotaro, Ashida, Yasunari, Uekusa, Hidehero, Guo, Fang and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2010. Selective transformation pathways between crystalline forms of an organic material established from powder X-ray diffraction analysis. Chemical Communications- Royal Society of Chemistry 46 (24) , pp. 4264-4266. 10.1039/C0CC00233J

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Abstract

The methanol solvate crystalline phase (M) of benzene-1,2,4,5-tetracarboxylic acid transforms selectively to a hydrate phase (H) or a non-solvate phase (N) depending on the presence of atmospheric water vapour; knowledge of the crystal structures of M and N, determined here using single-crystal and powder X-ray diffraction, respectively, yields insights into mechanistic aspects of the solid-state transformations.

Item Type:	Article
Status:	Published
Schools:	Advanced Research Computing @ Cardiff (ARCCA) Chemistry
Subjects:	Q Science > QD Chemistry
Publisher:	Royal Society of Chemistry
ISSN:	1359-7345
Last Modified:	18 Oct 2022 13:11
URI:	https://orca.cardiff.ac.uk/id/eprint/12819

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