Direct observation of a transient polymorph during crystallization

Hughes, Colan Evan and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2010. Direct observation of a transient polymorph during crystallization. Chemical Communications- Royal Society of Chemistry 46 (27) , pp. 4982-4984. 10.1039/C0CC01007C

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Abstract

Application of a technique developed for in situ solid-state 13C NMR studies of crystallization processes reveals direct evidence that crystallization of glycine from a methanol/water solution involves the initial transient formation of the β polymorph, which then undergoes a solution-mediated polymorphic transformation to yield the more stable α polymorph.

Item Type:	Article
Status:	Published
Schools:	Schools > Chemistry
Subjects:	Q Science > QD Chemistry
Publisher:	Royal Society of Chemistry
ISSN:	1359-7345
Last Modified:	18 Oct 2022 13:11
URI:	https://orca.cardiff.ac.uk/id/eprint/12821

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