Synthesis and characterization of nanoporous phospho-tungstate organic - inorganic hybrid materials

Rao, K. N., Dingwall, L. D., Gai, P. L., Lee, Adam Fraser, Tavener, S. J., Young, N. A. and Wilson, Karen 2008. Synthesis and characterization of nanoporous phospho-tungstate organic - inorganic hybrid materials. Journal of Materials Chemistry 18 (8) , pp. 868-874. 10.1039/b715826b

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Abstract

Nanoporous phospho-tungstate organic–inorganic hybrid materials have been synthesized from sodium tungstate and mono-n-dodecyl phosphate (MDP), which was used as both surfactant and phosphorus precursor. These hybrid materials were thoroughly characterized by N2 adsorption, elemental analysis, powder XRD, FTIR, Raman, TG, TEM and XPS and possess lamellar structures with interlayer spacings of 3.2 nm. A plausible method for formation of hybrid materials comprised of lacunary Keggin anions and micelles of surfactants is proposed.

Item Type:	Article
Date Type:	Publication
Status:	Published
Schools:	Chemistry Cardiff Catalysis Institute (CCI)
Subjects:	Q Science > QD Chemistry
ISSN:	0959-9428
Last Modified:	07 May 2023 21:50
URI:	https://orca.cardiff.ac.uk/id/eprint/12952

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