Synthesis of functionalized tetrahydrofuran derivatives from 2,5-dimethylfuran through cascade reactions

Li, J., Muller, E., Pera-Titus, M., Jérôme, F. and De Oliveira Vigier, K. 2019. Synthesis of functionalized tetrahydrofuran derivatives from 2,5-dimethylfuran through cascade reactions. Green Chemistry 21 (10) , pp. 2601-2609. 10.1039/C9GC01060B

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Abstract

A three-step strategy is proposed for the functionalization of the methyl group of 2,5-dimethylfuran, encompassing the ring opening of 2,5-dimethylfuran to 2,5-hexanedione, its further aldol condensation with aldehydes, and hydrogenation–cyclization of the condensation intermediate to generate alkylated tetrahydrofuran. Active and selective catalysts could be identified for the aldol condensation and hydrogenation–cyclization reactions.

Item Type:	Article
Date Type:	Publication
Status:	Published
Schools:	Schools > Chemistry Research Institutes & Centres > Cardiff Catalysis Institute (CCI)
Publisher:	Royal Society of Chemistry
ISSN:	1463-9262
Date of Acceptance:	24 March 2019
Last Modified:	12 Jan 2021 15:45
URI:	https://orca.cardiff.ac.uk/id/eprint/137473

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