Kariuki, Benson M.  ORCID: https://orcid.org/0000-0002-8658-3897, Abdel-Wahab, Bakr F., Mohamed, Hanan A. and El-Hiti, Gamal A. ORCID: https://orcid.org/0000-0001-6675-3126
2022.
Synthesis and structure determination of 2-cyano-3-(1-phenyl-3-(thiophen-2-yl)-1 H -pyrazol-4-yl)acrylamide.
Molbank
2022
(2)
, eM1372.
10.3390/m1372
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License URL: https://creativecommons.org/licenses/by/4.0/
Official URL: https://doi.org/10.3390/m1372
Abstract
2-Cyano-3-(1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-4-yl)acrylamide (3) was synthesized in 90% yield from condensation of equimolar equivalents of 1-phenyl-3-(thiophen-2-yl)-1H-pyrazole-4-carbaldehyde (1) and 2-cyanoacetamide (2) in boiling ethanol under basic condition for 45 min. The structure of 3 was determined using NMR spectroscopy and single crystal X-ray diffraction.
| Item Type: | Article |
|---|---|
| Date Type: | Published Online |
| Status: | Published |
| Schools: | Schools > Chemistry |
| Additional Information: | License information from Publisher: LICENSE 1: URL: https://creativecommons.org/licenses/by/4.0/ |
| Publisher: | MDPI |
| Date of First Compliant Deposit: | 1 June 2022 |
| Date of Acceptance: | 28 May 2022 |
| Last Modified: | 15 May 2023 21:35 |
| URI: | https://orca.cardiff.ac.uk/id/eprint/150194 |
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