A microwave-assisted synthesis of triphenodioxazines [TPDOs]

NajeebUllah, Muhammad, Knight, David William, Munawar, Munawar Ali, Yaseenx, Muhamad and Vincenzo, Fusillo 2010. A microwave-assisted synthesis of triphenodioxazines [TPDOs]. Tetrahedron 66 (34) , pp. 6761-6764. 10.1016/j.tet.2010.06.085

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Abstract

A convenient and efficient method for the synthesis of triphenodioxazines [TPDOs] 1 by oxidative cyclisation of 2,5-bis-(arylamino)-3,6-dichlorocyclohexa-2,5-diene-1,4-diones 6 using potassium persulfate as the oxidising agent in 95‑97% sulfuric acid triggered by microwave irradiation is described.

Item Type:	Article
Date Type:	Publication
Status:	Published
Schools:	Chemistry Cardiff Catalysis Institute (CCI)
Subjects:	Q Science > QD Chemistry
Publisher:	Elsevier
ISSN:	0040-4020
Last Modified:	06 May 2023 01:28
URI:	https://orca.cardiff.ac.uk/id/eprint/23074

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