Barium manganate in microwave-assisted oxidation reactions: synthesis of lactones by oxidative cyclization of diols

Bagley, Mark Christopher, Lin, Zhifan, Phillips, David J. and Graham, Andy 2009. Barium manganate in microwave-assisted oxidation reactions: synthesis of lactones by oxidative cyclization of diols. Tetrahedron Letters 50 (49) , pp. 6823-6825. 10.1016/j.tetlet.2009.09.117

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Abstract

Microwave irradiation of a range of diols at 150 °C in acetonitrile in the presence of three equivalents of barium manganate facilitates a novel tandem oxidation/heterocyclocondensation to give the corresponding lactone, including both small and medium ring lactones, in only one hour and in high yield without the need for chromatographic purification.

Item Type:	Article
Date Type:	Publication
Status:	Published
Schools:	Chemistry
Subjects:	Q Science > QD Chemistry
Publisher:	Elsevier
ISSN:	0040-4039
Last Modified:	19 Mar 2016 22:40
URI:	https://orca.cardiff.ac.uk/id/eprint/23693

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