Browse by All Cardiff Authors

Elliott, Mark C. ORCID: https://orcid.org/0000-0003-0132-0818, Gregory, Kasimir P., Hughes, Colan E. and Ward, Benjamin D. ORCID: https://orcid.org/0000-0003-1406-5940 2026. Exploring the interface of hyperconjugation and polarizability─enhancing pedagogies for charge stabilization in organic chemistry. Journal of Chemical Education 10.1021/acs.jchemed.6c00708

Elliott, Mark C. ORCID: https://orcid.org/0000-0003-0132-0818, Johnson, Edwin C., Gregory, Kasimir P. and Hughes, Colan. E. 2026. Rethinking the nature and extent of inductive effects in organic compounds. Journal of Chemical Education 103 (6) , pp. 3156-3164. 10.1021/acs.jchemed.6c00141

Smalley, Christopher J. H., Hughes, Colan E., Willhammar, Tom, Pandya, Raj, Saikin, Semion K., Johnstone, Duncan N., Gorman, Jeffrey, Sung, Jooyoung, Jacucci, Gianni, Midgley, Paul A., Kepaptsoglou, Demie M., Ramasse, Quentin M., Rao, Akshay, Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 and Collins, Sean M. 2026. Structural properties, polymorphism, and multiscale disorder unravel energy transport limitations in perylene diimide semiconductors. Science Advances 12 (22) , eaed0037. 10.1126/sciadv.aed0037

Wagner, Avital, Margalit, Noam, Fishman, Yahel, Indri, Shashanka S., Upcher, Alexander, Baranov, Mark, Nativ-Roth, Einat, Hughes, Colan E., Kariuki, Benson M. ORCID: https://orcid.org/0000-0002-8658-3897, Haataja, Johannes S., Schertel, Lukas, Yates, Jonathan R., Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598, Place, Allen R., Mojzes, Peter and Palmer, Benjamin A. 2026. Harnessing microalgae for the biosynthesis of molecular crystals. Nature Biotechnology 10.1038/s41587-026-03006-6

Chèvre, Romain, Hughes, Colan E., Cousin, Samuel F., Juramy, Marie, Ziarelli, Fabio, Viel, Stéphane, Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598, Mollica, Giulia and Thureau, Pierre 2026. New insights into the structural properties of calcium carbonate hemihydrate by NMR crystallography. Crystal Growth & Design 26 (3) , pp. 1291-1300. 10.1021/acs.cgd.5c01459

Kelly, Nicole L., Borthwick, Emma A. L., Lawrence, Gaynor B., Wheatley, Paul S., Karunathilake, Arosha A. K., Magdysyuk, Oxana V., Lloyd, David C., Hughes, Colan E., Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598, Morris, Russell E. and Ashbrook, Sharon E. 2026. Understanding the mechanism of nontraditional zeolite synthesis using in situ nuclear magnetic resonance spectroscopy and x-ray diffraction. Journal of the American Chemical Society 48 (1) , pp. 1478-1492. 10.1021/jacs.5c17807

Gauttier, Rose, Hughes, Colan E., Kariuki, Benson M. ORCID: https://orcid.org/0000-0002-8658-3897 and Harris, Kenneth D.M. ORCID: https://orcid.org/0000-0001-7855-8598 2025. In-situ solid-state NMR spectroscopy reveals competing crystallization pathways for a system that forms structurally diverse multicomponent crystalline phases. Solid State Nuclear Magnetic Resonance 140 , 102046. 10.1016/j.ssnmr.2025.102046

Elliott, Mark C. ORCID: https://orcid.org/0000-0003-0132-0818 and Hughes, Colan E. 2025. The interface of hybridization, hyperconjugation, and conformation in organic chemistry teaching. Journal of Chemical Education 102 (8) , pp. 3459-3467. 10.1021/acs.jchemed.5c00445

Harris, Kenneth D.M. ORCID: https://orcid.org/0000-0001-7855-8598 and Hughes, Colan E. 2025. NMR crystallization: The application of NMR strategies to monitor the evolution of crystallization processes. Bryce, David L., ed. Modern NMR Crystallography: Concepts and Applications, Vol. 36 New Developments in NMR, Royal Society of Chemistry, pp. 342-371. (10.1039/9781837673179-00342)

Kelly, Nicole L., Borthwick, Emma A. L., Lawrence, Gaynor B., Wheatley, Paul S., Hughes, Colan E., Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598, Morris, Russell E. and Ashbrook, Sharon E. 2025. Exploiting in situ NMR spectroscopy to understand non-traditional methods for zeolite synthesis. Chemical Science 16 (10) , pp. 4245-4255. 10.1039/d4sc07931k

Hughes, Colan E., Kariuki, Benson M. ORCID: https://orcid.org/0000-0002-8658-3897, Almetahr, Abrar, Saint-Mart, Jessica, Williams, Andrew, Samperisi, Laura and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2025. Solid-state structure of xanthine determined by a combination of 3D electron diffraction, powder x-ray diffraction, and DFT-D calculations. Crystal Growth and Design 25 (4) , pp. 895-902. 10.1021/acs.cgd.4c01717

Elliott, Mark C. ORCID: https://orcid.org/0000-0003-0132-0818, Hughes, Colan E., Knowles, Peter J. ORCID: https://orcid.org/0000-0003-4657-6331 and Ward, Benjamin D. ORCID: https://orcid.org/0000-0003-1406-5940 2025. Alkyl groups in organic molecules are NOT inductively electron-releasing. Organic and Biomolecular Chemistry 23 (2) , pp. 352-359. 10.1039/D4OB01572J

Hughes, Colan E., Ratnasingam, Naomi V., Williams, Andrew, Benhenou, Erwan, Patterson, Rhian and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2025. NMR crystallization: In-situ NMR strategies for monitoring the evolution of crystallization processes. Faraday Discussions 255 , pp. 520-552. 10.1039/D4FD00079J

Smalley, Christopher J. H., Hughes, Colan E., Hildebrand, Mariana, Aizen, Ruth, Bauer, Melanie, Yamano, Akihito, Levy, Davide, Mirsky, Simcha K., Shaked, Natan T., Young, Mark T. ORCID: https://orcid.org/0000-0002-9615-9002, Kolb, Ute, Gazit, Ehud, Kronik, Leeor and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2024. Understanding the solid-state structure of riboflavin through a multitechnique approach. Crystal Growth and Design 24 (15) , pp. 6256-6266. 10.1021/acs.cgd.4c00480

Wagner, Avital, Merkelbach, Johannes, Samperisi, Laura, Pinsk, Noam, Kariuki, Benson M. ORCID: https://orcid.org/0000-0002-8658-3897, Hughes, Colan E., Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 and Palmer, Benjamin A. 2024. Structure determination of biogenic crystals directly from 3D electron diffraction data. Crystal Growth and Design 24 (3) , pp. 899-905. 10.1021/acs.cgd.3c01290

Cousin, Samuel François, Hughes, Colan E., Ziarelli, Fabio, Viel, Stéphane, Mollica, Giulia, Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598, Pinon, Arthur C. and Thureau, Pierre 2023. Exploiting solid-state dynamic nuclear polarization NMR spectroscopy to establish the spatial distribution of polymorphic phases in a solid material. Chemical Science 14 , pp. 10121-10128. 10.1039/D3SC02063K

Al Rahal, Okba, Kariuki, Benson M. ORCID: https://orcid.org/0000-0002-8658-3897, Hughes, Colan E., Williams, P.Andrew, Xu, Xiaoyan, Gaisford, Simon, Iuga, Dinu and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2023. Unraveling the Complex Solid-State Phase Transition Behavior of 1-Iodoadamantane, a Material for Which Ostensibly Identical Crystals Undergo Different Transformation Pathways. Crystal Growth and Design 23 (5) , pp. 3820-3833. 10.1021/acs.cgd.3c00223

Dosso, Jacopo ORCID: https://orcid.org/0000-0003-4173-3430, Oubaha, Hamid, Fasano, Francesco, Melinte, Sorin, Gohy, Jean-François, Hughes, Colan E., Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598, Demitri, Nicola, Abrami, Michela, Grassi, Mario and Bonifazi, Davide ORCID: https://orcid.org/0000-0001-5717-0121 2022. Boron nitride-doped polyphenylenic organogels. Chemistry of Materials 34 (23) , pp. 10670-10680. 10.1021/acs.chemmater.2c01766

Smalley, Christopher, Hoskyns, Harriet E., Hughes, Colan E, Johnstone, Duncan N., Willhammar, Tom, Young, Mark T. ORCID: https://orcid.org/0000-0002-9615-9002, Pickard, Chris J., Logsdail, Andrew J. ORCID: https://orcid.org/0000-0002-2277-415X, Midgley, Paul and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2022. A structure determination protocol based on combined analysis of 3D-ED data, powder XRD data, solid-state NMR data and DFT-D calculations reveals the structure of a new polymorph of L-tyrosine. Chemical Science 13 (18) , pp. 5277-5288. 10.1039/D1SC06467C

Pinsk, Noam, Wagner, Avital, Cohen, Lilian, Smalley, Christopher J. H., Hughes, Colan E., Zhang, Gan, Pavan, Mariela J., Casati, Nicola, Jantschke, Anne, Goobes, Gil, Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 and Palmer, Benjamin A. 2022. Biogenic guanine crystals are solid solutions of guanine and other purine metabolites. Journal of the American Chemical Society 144 (11) , pp. 5180-5189. 10.1021/jacs.2c00724

Smalley, Christopher J. H., Logsdail, Andrew J. ORCID: https://orcid.org/0000-0002-2277-415X, Hughes, Colan E., Iuga, Dinu, Young, Mark T. ORCID: https://orcid.org/0000-0002-9615-9002 and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2022. Solid-state structural properties of alloxazine determined from powder XRD data in conjunction with DFT-D calculations and solid-state NMR spectroscopy: unraveling the tautomeric identity and pathways for tautomeric interconversion. Crystal Growth and Design 22 (1) , pp. 524-534. 10.1021/acs.cgd.1c01114

Al Rahal, Okba, Williams, P. Andrew, Hughes, Colan E., Kariuki, Benson M. ORCID: https://orcid.org/0000-0002-8658-3897 and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2021. Structure determination of multicomponent crystalline phases of (S)-Ibuprofen and l-Proline from powder x-ray diffraction data, augmented by complementary experimental and computational techniques. Crystal Growth and Design 21 (4) , pp. 2498-2507. 10.1021/acs.cgd.1c00160

Jones, Corey L., Hughes, Colan E., Yeung, Hamish H.-M., Paul, Alison ORCID: https://orcid.org/0000-0002-7653-9964, Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 and Easun, Timothy L. ORCID: https://orcid.org/0000-0002-0713-2642 2021. Exploiting in-situ NMR to monitor the formation of a metal-organic framework. Chemical Science 12 (4) , pp. 1486-1494. 10.1039/D0SC04892E

Sun, Tu, Hughes, Colan E., Guo, Linshuo, Wei, Lei, Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598, Zhang, Yue-Biao and Ma, Yanhang 2020. Direct-space structure determination of covalent organic frameworks from 3D electron diffraction data. Angewandte Chemie International Edition 59 (50) , pp. 22638-22644. 10.1002/anie.202009922

Schotten, Christiane, Leprevost, Samy K., Yong, Low Ming, Hughes, Colan E., Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 and Browne, Duncan L. ORCID: https://orcid.org/0000-0002-8604-229X 2020. Comparison of the thermal stabilities of diazonium salts and their corresponding triazenes. Organic Process Research and Development 24 (10) , pp. 2336-2341. 10.1021/acs.oprd.0c00162

Yan, Yuncheng, Kariuki, Benson M. ORCID: https://orcid.org/0000-0002-8658-3897, Hughes, Colan E., Logsdail, Andrew J. ORCID: https://orcid.org/0000-0002-2277-415X and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2020. Polymorphism in a multicomponent crystal system of trimesic acid and t-butylamine. Crystal Growth and Design 20 (9) , pp. 5736-5744. 10.1021/acs.cgd.0c00163

Dosso, Jacopo ORCID: https://orcid.org/0000-0003-4173-3430, Battisti, Tommaso, Ward, Benjamin D. ORCID: https://orcid.org/0000-0003-1406-5940, Demitri, Nicola, Hughes, Colan E., Williams, P. Andrew, Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 and Bonifazi, Davide ORCID: https://orcid.org/0000-0001-5717-0121 2020. Boron-nitrogen-doped nanographenes: a synthetic tale from borazine precursors. Chemistry - A European Journal 26 (29) , pp. 6608-6621. 10.1002/chem.201905794

Bemmer, Victoria, Bowker, Michael ORCID: https://orcid.org/0000-0001-5075-1089, Carter, James H., Davies, Philip R. ORCID: https://orcid.org/0000-0003-4394-766X, Edwards, Lee E. ORCID: https://orcid.org/0000-0003-2200-9578, Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598, Hughes, Colan E., Robinson, Fiona, Morgan, David J. ORCID: https://orcid.org/0000-0002-6571-5731 and Thomas, Matthew G. 2020. Rationalization of the X-ray photoelectron spectroscopy of aluminium phosphates synthesized from different precursors. RSC Advances 10 (14) , p. 84448452. 10.1039/C9RA08738A

Al Rahal, Okba, Hughes, Colan E., Williams, P. Andrew, Logsdail, Andrew J. ORCID: https://orcid.org/0000-0002-2277-415X, Diskin-Posner, Yael and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2019. Polymorphism of L-tryptophan. Angewandte Chemie International Edition 58 (52) , pp. 18788-18792. 10.1002/anie.201908247

Hughes, Colan E., Walkley, Brant, Gardner, Laura J., Walling, Samuel A., Bernal, Susan A., Iuga, Dinu, Provis, John L. and Harris, Kenneth D.M. ORCID: https://orcid.org/0000-0001-7855-8598 2019. Exploiting in-situ solid-state NMR spectroscopy to probe the early stages of hydration of calcium aluminate cement. Solid State Nuclear Magnetic Resonance 99 , -. 10.1016/j.ssnmr.2019.01.003

Vioglio, Paolo Cerreia, Thureau, Pierre, Juramy, Marie, Ziarelli, Fabio, Viel, Stéphane, Williams, P. Andrew, Hughes, Colan E., Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 and Mollica, Giulia 2019. A strategy for probing the evolution of crystallization processes by low-temperature solid-state NMR and dynamic nuclear polarization. Journal of Physical Chemistry Letters 10 (7) , pp. 1505-1510. 10.1021/acs.jpclett.9b00306

Zhou, Yating, Patterson, Rhian, Williams, P. Andrew, Kariuki, Benson M. ORCID: https://orcid.org/0000-0002-8658-3897, Hughes, Colan E., Samanta, Ranita, Devarapalli, Ramesh, Reddy, C. Malla, Apperley, David C. and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2019. Temperature-dependent structural properties, phase transition behavior, and dynamic properties of a benzene derivative in the solid state. Crystal Growth and Design 19 (4) , pp. 2155-2162. 10.1021/acs.cgd.8b01775

Hughes, Colan E, Williams, Andrew, Kariuki, Benson M ORCID: https://orcid.org/0000-0002-8658-3897 and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2018. Establishing the transitory existence of amorphous phases in crystallization pathways by the CLASSIC NMR technique. ChemPhysChem 19 (24) , pp. 3341-3345. 10.1002/cphc.201800976

Khoj, Manal A., Hughes, Colan E., Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 and Kariuki, Benson M. ORCID: https://orcid.org/0000-0002-8658-3897 2018. Polymorphic phase transformations of 3-chloro-trans-cinnamic acid and its solid solution with 3-bromo-trans-cinnamic acid. Acta Crystallographica Section C: Structural Chemistry 74 (8) , pp. 923-928. 10.1107/S2053229618009269

Cerreia Vioglio, Paolo, Mollica, Giulia, Juramy, Marie, Hughes, Colan E., Williams, P. Andrew, Ziarelli, Fabio, Viel, Stéphane, Thureau, Pierre and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2018. Insights into the crystallization and structural evolution of glycine dihydrate by in situ solid-state NMR spectroscopy. Angewandte Chemie International Edition 57 (22) , pp. 6619-6623. 10.1002/anie.201801114

Hughes, Colan Evan, Boughdiri, Ines, Bouakkaz, Clement, Williams, Philip Andrew and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2018. Elucidating the crystal structure of DL-Arginine by combined powder X-ray diffraction data analysis and periodic DFT-D calculations. Crystal Growth and Design 18 (1) , pp. 42-46. 10.1021/acs.cgd.7b01412

Maruyoshi, Keisuke, Iuga, Dinu, Watts, Abigail E., Hughes, Colan E., Harris, Kenneth D.M. ORCID: https://orcid.org/0000-0001-7855-8598 and Brown, Steven P. 2017. Assessing the detection limit of a minority solid-state Form of a pharmaceutical by 1 H double-quantum magic-angle spinning nuclear magnetic resonance spectroscopy. Journal of Pharmaceutical Sciences 106 (11) , pp. 3372-3377. 10.1016/j.xphs.2017.07.014

Zilka, Miri, Dudenko, Dmytro V, Hughes, Colan, Williams, Philip, Sturniolo, Simone, Franks, W. Trent, Pickard, Chris J., Yates, Jonathan R., Harris, Kenneth ORCID: https://orcid.org/0000-0001-7855-8598 and Brown, Steven P. 2017. Ab initio random structure searching of organic molecular solids: assessment and validation against experimental data. Physical Chemistry Chemical Physics 19 (38) , pp. 25949-25960. 10.1039/C7CP04186A

Hughes, Colan E., Reddy, G. N. Manjunatha, Masiero, Stefano, Brown, Steven P., Williams, P. Andrew and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2017. Determination of a complex crystal structure in the absence of single crystals: analysis of powder X-ray diffraction data, guided by solid-state NMR and periodic DFT calculations, reveals a new 2'-deoxyguanosine structural motif. Chemical Science 8 (5) , pp. 3971-3979. 10.1039/C7SC00587C

Harris, Kenneth D.M. ORCID: https://orcid.org/0000-0001-7855-8598, Hughes, Colan, Williams, Philip Andrew and Edwards-Gau, Gregory R. 2017. `NMR Crystallization': in-situ NMR techniques for time-resolved monitoring of crystallization processes. Acta Crystallographica Section C Structural Chemistry C73 (3) , pp. 137-148. 10.1107/S2053229616019811

Khoj, Manal A, Hughes, Colan Evan, Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 and Kariuki, Benson ORCID: https://orcid.org/0000-0002-8658-3897 2017. Structural diversity of solid solutions formed between 3-chloro-trans-cinnamic acid and 3-bromo-trans-cinnamic acid. Crystal Growth and Design 17 (3) , pp. 1276-1284. 10.1021/acs.cgd.6b01675

Palmer, Benjamin A., Collins, Stephen P., Hulliger, Juerg, Hughes, Colan E. and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2016. Determining molecular orientations in disordered materials from X-ray linear dichroism at the iodine L1-edge. Journal of the American Chemical Society 138 (50) , pp. 16188-16191. 10.1021/jacs.6b09054

Hughes, Colan Evan and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2016. Calculation of solid-state NMR Lineshapes using contour analysis. Solid State Nuclear Magnetic Resonance 80 , pp. 7-13. 10.1016/j.ssnmr.2016.10.002

Williams, Philip Andrew, Hughes, Colan Evan, Martin, Jean, Courvoisier, Emilie, Buanz, Asma B. M., Gaisford, Simon and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2016. Understanding the solid-state hydration behavior of a common amino acid: identification, structural characterization, and hydration/dehydration processes of new hydrate phases of l-lysine. Journal of Physical Chemistry C 120 (17) , pp. 9385-9392. 10.1021/acs.jpcc.5b12420

Watts, Abigail E., Maruyoshi, K, Hughes, Colan Evan, Brown, S and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2016. Combining the advantages of powder X-ray diffraction and NMR crystallography in structure determination of the pharmaceutical material cimetidine hydrochloride. Crystal Growth and Design 16 (4) , pp. 1798-1804. 10.1021/acs.cgd.6b00016

Williams, Eleri, Brousseau, Emmanuel ORCID: https://orcid.org/0000-0003-2728-3189, Lavery, Nick, Mehraban, Shahin, Keast, Victoria, Hughes, Colan and Harris, Kenneth ORCID: https://orcid.org/0000-0001-7855-8598 2016. Nanosecond laser milling of the amorphous alloy Zr41.2Ti13.8Cu12.5Ni10Be22.5. Presented at: 11 th International Conference on Multi-Material Micro Manufacture (4M2016), co-organised with 10th International Workshop on Microfactories (IWMF2016), Lyngby, Denmark,, 13-15 September 2016.

Zhou, Yating, Guo, Fang, Hughes, Colan Evan, Browne, Duncan L. ORCID: https://orcid.org/0000-0002-8604-229X, Peskett, Thomas R. and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2015. Discovery of new metastable polymorphs in a family of urea co-crystals by solid-state mechanochemistry. Crystal Growth and Design 15 (6) , pp. 2901-2907. 10.1021/acs.cgd.5b00331

Williams, P. Andrew, Hughes, Colan E. and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2015. L-lysine: exploiting powder X-ray diffraction to complete the set of crystal structures of the 20 directly encoded proteinogenic amino acids. Angewandte Chemie International Edition 54 (13) , pp. 3973-3977. 10.1002/anie.201411520

Shivakumar, Kilingaru I., Yan, Yuncheng, Hughes, Colan Evan, Apperley, David C., Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 and Sanjayan, Gangadhar J. 2015. Exploiting powder X-ray diffraction to establish the solvent-assisted solid-state supramolecular assembly of pillar[5]quinone. Crystal Growth and Design 15 (4) , pp. 1583-1587. 10.1021/acs.cgd.5b00277

Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598, Hughes, Colan Evan and Williams, P. Andrew 2015. Monitoring the evolution of crystallization processes by in-situ solid-state NMR spectroscopy. Solid State Nuclear Magnetic Resonance 65 , pp. 107-113. 10.1016/j.ssnmr.2014.11.004

Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598, Hughes, Colan and Williams, Philip Andrew 2015. In situ solid-state NMR studies of crystallization processes. Advances in Organic Crystal Chemistry , pp. 31-53. 10.1007/978-4-431-55555-1_3

Hughes, Colan Evan, Williams, Andrew, Keast, Victoria, Charalampopoulos, Vasileios, Edwards-Gau, Gregory R. and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2015. New in situ solid-state NMR techniques for probing the evolution of crystallization processes: pre-nucleation, nucleation and growth. Faraday Discussions 179 , pp. 115-140. 10.1039/C4FD00215F

Hughes, Colan E., Williams, P. Andrew and Harris, Kenneth D. M. ORCID: https://orcid.org/0000-0001-7855-8598 2014. "Classic NMR": an in-situ NMR strategy for mapping the time-evolution of crystallization processes by combined liquid-state and solid-state measurements. Angewandte Chemie International Edition 53 (34) , pp. 8939-8943. 10.1002/anie.201404266

Iwama, Sekai, Kuyama, Kazunori, Mori, Yuko, Manoj, Kochunnoonny, Gonnade, Rajesh G., Suzuki, Katsuaki, Hughes, Colan Evan, Williams, Philip Andrew, Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598, Veesler, Stéphane, Takahashi, Hiroki, Tsue, Hirohito and Tamura, Rui 2014. Highly efficient chiral resolution of dl-arginine by cocrystal formation followed by recrystallization under preferential-enrichment conditions. Chemistry - a European Journal 20 (33) , pp. 10343-10350. 10.1002/chem.201402446

Sharples, Katherine Mary, Carter, Emma ORCID: https://orcid.org/0000-0001-6691-2377, Hughes, Colan Evan, Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598, Platts, James Alexis ORCID: https://orcid.org/0000-0002-1008-6595 and Murphy, Damien Martin ORCID: https://orcid.org/0000-0002-5941-4879 2013. An ENDOR and DFT analysis of hindered methyl group rotations in frozen solutions of bis(acetylacetonato)-copper(ii). Physical Chemistry Chemical Physics 15 (36) , pp. 15214-15222. 10.1039/c3cp52464g

Dudenko, Dmytro, Williams, Philip Andrew, Hughes, Colan Evan, Antzutkin, Oleg N., Velaga, Sitaram P., Brown, Steven P. and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2013. Exploiting the synergy of powder X-ray diffraction and solid-state NMR spectroscopy in structure determination of organic molecular solids. The Journal of Physical Chemistry C 117 (23) , pp. 12258-12265. 10.1021/jp4041106

Williams, Philip Andrew, Hughes, Colan Evan, Buanz, Asma B. M., Gaisford, Simon and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2013. Expanding the Solid-State Landscape ofl-Phenylalanine: Discovery of Polymorphism and New Hydrate Phases, with Rationalization of Hydration/Dehydration Processes. The Journal of Physical Chemistry C 117 (23) , pp. 12136-12145. 10.1021/jp401547f

Khoj, Manal A., Hughes, Colan Evan, Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 and Kariuki, Benson ORCID: https://orcid.org/0000-0002-8658-3897 2013. Polymorphism in a trans-cinnamic acid derivative exhibiting two distinct β‑type phases: structural properties, [2 + 2] photodimerization reactions, and polymorphic phase transition behavior. Crystal Growth and Design 13 (9) , pp. 4110-4117. 10.1021/cg4009202

Yan, Yuncheng, Hughes, Colan Evan, Kariuki, Benson ORCID: https://orcid.org/0000-0002-8658-3897 and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2013. A rare case of polymorphism in a three-component co-crystal system, with each polymorph having ten independent molecules in the asymmetric unit. Crystal Growth and Design 13 (1) , pp. 27-30. 10.1021/cg3016035

Williams, Philip Andrew, Hughes, Colan Evan and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2012. New insights into the preparation of the low-melting polymorph of racemic ibuprofen. Crystal Growth and Design 12 (12) , pp. 5839-5845. 10.1021/cg300599q

Hughes, Colan Evan, Williams, Philip Andrew, Peskett, Thomas Roper and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2012. Exploiting in situ solid-state NMR for the discovery of new polymorphs during crystallization processes. The Journal of Physical Chemistry Letters 3 (21) , pp. 3176-3181. 10.1021/jz301252u

Williams, Philip Andrew, Hughes, Colan Evan, Lim, Gin Keat, Kariuki, Benson ORCID: https://orcid.org/0000-0002-8658-3897 and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2012. Discovery of a New System Exhibiting Abundant Polymorphism: m-Aminobenzoic Acid. Crystal Growth & Design 12 (6) , pp. 3104-3113. 10.1021/cg3003178

Courvoisier, Emilie, Williams, Philip Andrew, Lim, Gin Keat, Hughes, Colan Evan and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2012. The crystal structure of l-arginine. Chemical Communications 48 (22) , pp. 2761-2763. 10.1039/c2cc17203h

Aliev, Abil E., Mann, Sam E., Iuga, Dinu, Hughes, Colan Evan and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2011. Natural-abundance solid-state H-2 NMR spectroscopy at high magnetic field. Journal of Physical Chemistry A 115 (22) , pp. 5568-5578. 10.1021/jp202810k

Marti-Rujas, Javier, Kariuki, Benson ORCID: https://orcid.org/0000-0002-8658-3897, Hughes, Colan Evan, Morte-Ródenas, Anabel, Guo, Fang, Glavcheva-Laleva, Zornitza, Tastemur, Kemal, Ooi, Liling, Yeo, Lily and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2011. Structural diversity, but no polymorphism, in a homologous family of co-crystals of urea and α,ω-dihydroxyalkanes. New Journal of Chemistry 35 (7) , pp. 1515-1521. 10.1039/C1NJ20040B

Palmer, Benjamin Alexander, Kariuki, Benson ORCID: https://orcid.org/0000-0002-8658-3897, Muppidi, Vamsee Krishna, Hughes, Colan Evan and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2011. An incommensurate thiourea inclusion compound. Chemical Communications- Royal Society of Chemistry 47 (13) , pp. 3760-3762. 10.1039/C0CC05477A

Aliev, Abil E., Mann, Sam E., Rahman, Aisha S., McMillan, Paul F., Corà, Furio, Iuga, Dinu, Hughes, Colan Evan and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2011. High-resolution solid-state 2H NMR spectroscopy of polymorphs of glycine. Journal of Physical Chemistry A 115 (44) , pp. 12201-12211. 10.1021/jp207592u

Hughes, Colan Evan and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2010. Direct observation of a transient polymorph during crystallization. Chemical Communications- Royal Society of Chemistry 46 (27) , pp. 4982-4984. 10.1039/C0CC01007C

Hughes, Colan Evan and Harris, Kenneth David MacLean ORCID: https://orcid.org/0000-0001-7855-8598 2009. The effect of deuteration on polymorphic outcome in the crystallization of glycine from aqueous solution. New Journal of Chemistry 33 (4) , pp. 713-716. 10.1039/B819199A

Hughes, Colan Evan and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2008. A technique for in situ monitoring of crystallization from solution by solid-state C-13 CPMAS NMR spectroscopy. Journal of Physical Chemistry A 112 (30) , pp. 6808-6810. 10.1021/jp805182v

Olejniczak, S., Mikua-Pacboczyk, J., Hughes, Colan Evan and Potrzebowski, M. J. 2008. N-15 and C-13 high-resolution solid-state NMR study of the polymorphism of the L-enantiomer of N-benzoylphenylalanine. Journal of Physical Chemistry B 112 (6) , pp. 1586-1593. 10.1021/jp073428u

Olejniczak, S., Mikua-Pacboczyk, J., Hughes, Colan Evan and Potrzebowski, M. J. 2008. 15N and13C high-resolution solid-state NMR study of the polymorphism of the L-enantiomer of N-benzoylphenylalanine. Journal of Physical Chemistry B 112 (6) , pp. 1586-1593. 10.1021/jp073428u

Hamad, S., Hughes, Colan Evan, Catlow, C. R. A. and Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2008. Clustering of glycine molecules in aqueous solution studied by molecular dynamics simulation. Journal of Physical Chemistry B 112 (24) , pp. 7280-7288. 10.1021/jp711271z

Hughes, Colan Evan, Hamad, Said, Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598, Catlow, C. Richard A. and Griffiths, Peter Charles 2007. A multi-techuique approach for probing the evolution of structural properties during crystallization of organic materials from solution. Faraday Discussions- Royal Society of Chemistry 136 , pp. 71-89. 10.1039/B616611C